NurdRage
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Lab Notes - Failure in Making Sodium Nitrite
🕑 Added 2023-10-19 18:45:51 +0000 UTCFinal version. As usual, i'll post on Saturday, but you all get to see it now :)
Comments
NurdRage
its something to a consider. the issue is that such solvents aren't easy to come by for the amateur. but it's definitely something to try.
Twizzy
For the direct hydrolysis, would an aprotic solvent help? Maybe a slow addition to DMSO with a carbonate, or maybe even CaO. Alternately, it might be possible to combine the acid directly with powdered CaO or MgO and a bit of heat to melt it.
NurdRage
yep, of course now the question becomes what sort of interesting diazo compounds can i make? hehehe, i'll see
Mono Keras
Can’t isopropyl nitrite be used to make sodium azide? Which in its way is also a useful reagent to get diazo compounds
